Penetration Grade

The penetration test of bitumen quantifies the hardness or softness of bitumen by measuring the depth of penetration of standard loaded needle in five seconds while maintaining bitumen sample temperature at 25 °C. The more viscous the bitumen, the less distance needle is able to penetrate. Hence, the penetration value for viscous bitumen is less.
For instance, if the needle penetrates between 6 and 7 mm in 5 seconds, we will have 60/70 bitumen.
The penetration is measured to specify the bitumen type in accordance with the climatic conditions of the area of bitumen consumption.
This penetration depth is empirically (albeit only roughly) correlated with asphalt binder performance. Therefore, asphalt binders with high penetration numbers (called “soft”) are used for cold climates (like 85/100) while asphalt binders with low penetration numbers (called “hard”) are used for warm climates (like 40/50).

Test
Method
30-40
40-50
60-70
85-100
100-120
200-300
Specific gravity @25/25C ASTM D70 1/01-1/06 1/01-1/06 1/01-1/06 1/01-1/05 1/01-1/04 0.99-1/04
Penetration ,25°c,100g 5s,min ASTM D5 30-40 40-50 60-70 85-100 100-120 200-300
Softening point °C ASTM D-36 55-63 52-60 49-56 45-52 42-49 32min
Ductility ,25°c,5cm/min/cm ASTM D-113 100 min 100 min 100 min 100 min 100 min 100 min
Flash Point °C ASTM-D92 250 min 250 min 250 min 230 min 250 min 177min
Solubility in trichloroethylene (min %) ASTM-D2042 99.5 min 99.5 min 99.5 min 99.5 min 99.5 min 99.0min
Spot test A.A.S.H.T.T102 Negative Negative Negative Negative Negative Negative
Drop in penetration after heating% ASTM-D5&D6 20 max 20 max 20 max 20 max 20 max 37min
Loss on heating(%wt) ASTM-D6 0.2 max 0.2 max 0.2 max 0.5 max 0.2 max 1max